Ji, ChangBeebower, Michael Lee2010-07-052012-02-242010-05Beebower, M. L. (2010). Electrochemical reduction of 1-bromooctane catalyzed by a dicobalt complex (Unpublished thesis). Texas State University-San Marcos, San Marcos, Texas.https://hdl.handle.net/10877/3277A dicobalt complex [CoII2L] has been synthesized according to previous methods. 1,2 The [CoII2L] complex-catalyzed electrochemical reduction of 1-bromooctane was investigated in dimethylformamide (DMF) using cyclic voltammetry (CV) in comparison to the corresponding non-catalyzed reduction. Due to the presence of atmospheric oxygen in the electrochemical cell, degradation of the dicobalt [CoII2L] catalyst occurred and catalytic reduction of 1-bromooctane could not be accurately characterized. Further research would include repeating the synthesis of the dicobalt complex [CoII2L] with greater purity standards and the use of an electrochemical cell fitted with a rubber septum(s) to prevent oxygen contamination.Text46 pages1 file (.pdf)enelectrochemical reductionI-bromooctanedicobaltcyclic voltammetrycatalystorganobromidealkyl halideligandHonors College